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Selected lectures - XRF

​Lectures on x-ray spectroscopy techniques

XRF_01_Fundamenta​ls

PDF version

This lecture provides a general introduction to XRF, including:

  • Some milestones in the history of x-rays
  • The nature of x-rays
  • Mechanisms of x-ray production
  • Interaction of x-rays with matter
  • The fitness of the method for qualitative and quantitative analysis
  • General considerations
  • Examples of application


XRF_02_Instrumentation for XRF

PDF version​

This lecture provides a general introduction to main hardware used for XRF spectroscopy, including:

  • Main configurations of XRF spectrometers
  • Excitation sources
  • Modifiers of x-ray beams
  • X-ray detectors
  • Signal processing

XRF_03_Comparison of WDXRF and EDXRF

PDF version

This lecture provides a comparison of the two main configurations used for XRF spectroscopy, including:

  • Excitation sources and modifiers
  • Principle of detection
  • Components and features of performance

 

 

 


XRF_04_Statistics and Detection Limits in XRF

PDF version​

This lecture provides a general refreshment of statistical concepts and recommendations for 

applicability in XRF spectroscopy, including:

  • Distributions
  • Recommendations to calculate DLs

XRF_05_EDXRF spectrum fitting algorithms and software

PDF version

This lecture introduces the algorithms used for peak and background fitting in XRF spectra:

  • Basic and advanced models
  • Available software packages

 



XRF_06_Introduction to XRF quantitative methods

PDF version

This lecture provides a general introduction to quantitative anbalysis in XRF, including:

  • Fundamentals
  • Common approaches followed

XRF_07_Method validation and QC in XRF

PDF version

This lecture provides general recommendations to improve the quality of measurement results, including:

  • Recommendations for method validation
  • Internal Quality Control actions
  • External QC


Assessing 2D spatial distribution of elements using FFXRF

Video recording:

Language: English

This lecture contains information on fundamentals of Full-field XRF analysis, including:

  • Concept
  • Main figures of performance
  • Examples of application

Assessing distribution of elements using micro and confocal XRF

Video recording:​

Language: English

This lecture contains information on fundamentals of Full-field XRF analysis, including:

  • Concept
  • Main figures of performance
  • Examples of application
micro and CXRF.jpg
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SXRF for CH.jpg
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Synchrotron techniques to support characterization of 

Cultural Heritage

PDF version​

This lecture introduces the use of synchrotron techniques to characterize objects from cultural, including:

  • Description of the synchrotron and beamlines
  • Techniques and their complementarity
  • Examples of application
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Transportable XRF and XRD scanners to support characterization of Cultural Heritage

Video recording:

Language: English

This lecture introduces the use of XRF and XRD transportable devices to characterize objects from cultural, including:

  • Fundamentals of the techniques
  • Description of the developed instruments
  • Examples of application
​TranspXRF-XRD.jpg

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XAS for CH.jpg
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X-ray absorption spectroscopy in support of 

characterization of cultural heritage

Video recording:​

​Language: English

This lecture introduces the use of XAS techniques to characterize objects from cultural, including:

  • Fundamentals
  • XANES and EXAFS
  • Examples of application

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GEXRF for the analysis of layered materials

PDF version​

This lecture introduces the use of Grazing Emission XRF to characterize layered materials:

  • Fundamentals
  • Examples of application


​GEXRF.jpg
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PIXE.jpg
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PIXE analysis

​​Video recording​:

​Language: English

This lecture introduces the use of PIXE as non-destructive technique to characterize 

​valuable objects, including:

  • Fundamentals
  • Practical recommendations
  • Examples of application


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